[ Synthèse de nouveaux dérivés γ-lactames assistée par micro-ondes en milieu sec: comparaison à la méthode classique de chauffage à reflux ]
Volume 20, Issue 4, July 2017, Pages 1221–1225
Ahmad Oubair1, Rachid Fihi2, and Driss Chebabe3
1 Département de chimie, Université My Smail Meknes, Faculté des Sciences et Technique, Errachidia, Morocco
2 Département de chimie, Université My Smail Meknes, Faculté des Sciences et Technique, Errachidia, Morocco
3 Laboratoire des Substances Naturelles & Synthèse et Dynamique Moléculaire, Département de chimie, Université My Smail Meknes, Faculté des Sciences et Technique, Errachidia, Morocco
Original language: French
Copyright © 2017 ISSR Journals. This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.
New γ-lactam derivatives are synthesized with good yields on a mineral support in "dry" medium and under microwave irradiations in a domestic furnace. The structures of the various products are established using 1HNMR, 13CNMR and IR spectroscopy.
Author Keywords: α-arylidene-γ-butyrolactone, chlorhydrate d’hydroxylamine, γ-lactames derivatives, microwave, silice.
Volume 20, Issue 4, July 2017, Pages 1221–1225
Ahmad Oubair1, Rachid Fihi2, and Driss Chebabe3
1 Département de chimie, Université My Smail Meknes, Faculté des Sciences et Technique, Errachidia, Morocco
2 Département de chimie, Université My Smail Meknes, Faculté des Sciences et Technique, Errachidia, Morocco
3 Laboratoire des Substances Naturelles & Synthèse et Dynamique Moléculaire, Département de chimie, Université My Smail Meknes, Faculté des Sciences et Technique, Errachidia, Morocco
Original language: French
Copyright © 2017 ISSR Journals. This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.
Abstract
New γ-lactam derivatives are synthesized with good yields on a mineral support in "dry" medium and under microwave irradiations in a domestic furnace. The structures of the various products are established using 1HNMR, 13CNMR and IR spectroscopy.
Author Keywords: α-arylidene-γ-butyrolactone, chlorhydrate d’hydroxylamine, γ-lactames derivatives, microwave, silice.
Abstract: (french)
De nouveaux dérivés γ-lactames sont synthétisés avec de bons rendements sur support minéral en ‘’milieu sec’’ et sous irradiations micro-ondes dans un four domestique. Les structures des différents produits sont établies par les méthodes spectroscopiques usuelles (RMN 1H, 13C et IR).
Author Keywords: α-arylidène-γ-lactones, chlorhydrate d’hydroxylamine, dérivés γ-lactames, micro-ondes, silice.
How to Cite this Article
Ahmad Oubair, Rachid Fihi, and Driss Chebabe, “Microwave synthesis of new γ-lactames derivatives in dry media: comparison with the conventional reflux heating method,” International Journal of Innovation and Applied Studies, vol. 20, no. 4, pp. 1221–1225, July 2017.
